Keywords

molten salt, voltammetry, concentration prediction, nuclear fuel reprocessing, electrorefining

Abstract

Normal pulse voltammetry was performed on LiCl-KCl-UCl3- MgCl2 molten salt mixtures while varying parameters such as pulse time, relaxation potential, and interval time. Concentrations of UCl3 up to 7 wt% were tested with a fixed 1.5 wt% MgCl2 concentration. The correlation between diffusion limited partial current density to UCl3 concentration exhibited an excellent fit to a 2nd order polynomial. A similar fit was obtained for the correlation between MgCl2 concentration and the diffusion limited partial current density at a fixed UCl3 concentration of 1.0 wt%.

Original Publication Citation

Zhang, C., Rappleye, D., & Simpson, M. F. (2016). Development and Optimization of Voltammetry for Real Time Analysis of Multi-Component Electrorefiner Salt. ECS Transactions, 75, 95. https://doi.org/10.1149/07515.0095ecst

Document Type

Conference Paper

Publication Date

2016-10

Publisher

IOP Publishing Ltd.

Language

English

College

Ira A. Fulton College of Engineering

Department

Chemical Engineering

University Standing at Time of Publication

Assistant Professor

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